Synthesis and structural characterization of single and mixed ligand complexes some group IIIA metal cations

Within the scope of this thesis, Aluminum (Al) and Indium (In) metal cations in Group 3A with +3 oxidation state were mixed with the acesulfame ligand as a single ligand and mixed ligand containing acesulfame-nicotinamide/N,N'- diethylnicotinamide and 1,10-phenanthroline complex structures. Compositions of the synthesized mixed ligand complexes were characterized by elemental analysis, FT-IR, UV-Vis and GC spectroscopy techniques as well as TGA / DTA / DrTGA analysis were studied. As an artificial sweetener molecule, acesulfame ligand which is often used in the industry, is a valuable ligand in coordination chemistry, owing to the many active groups that are involved in the structure of it. It is also a ligand that is easy to work with the ability to form precipitated solid material to obtain a single crystal in complex structures. There are studies in the literature mostly obtained with transition metals, but these studies with earth elements have not been found yet. Literature contribution and characterization studies of the structures to be obtained and studies can be used for industry are important. Keywords: Acesulfame, Nicotinamide, 1,10-phenantroline, N,N-diethylnicotinamide.