Synthesis and characterization of imine polymers containing aliphatic and aromatic groups
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Abstract (EN)
The oxidative polycondensation reaction conditions of 2,2?-[(2,5-dichloro-1,4-phenylene) bisnitrilomethylylidene]diphenol were examined between 40-90°C temperature in a aquaus alkaline medium. NaOCl, H2O2 and air oxygen were used as oxidants in reactions. Synthesized polymer of 2,2?-piperazine-1,4-diylbis[propane-3,1-diylnitrilomethylylidene]diphenol with graft polycondensation method. And its Schiff base-metal complexes were synthesized with Cu+2, Co+2, Ni+2, Cd+2, Zn+2, Pb+2 ve U+2 metal salts. Both the structures and properties of oligomer, polymer and monomers were characterized by spectral techniques, conductivity and cyclic voltametry (CV). Thermal properties of all synthesized compounds were determined by TGA-DTA analysis. Molecular weight of the oligomer was calculated by SEC analysis.
Author
Seçil Uysal
How to Cite
Seçil Uysal (Master Thesis). Synthesis and characterization of imine polymers containing aliphatic and aromatic groups, 2009, Çanakkale Onsekiz Mart University.
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