Catalytic synthesis of vitamin K3 (2-methyl-1,4-naphthoquinone)
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Abstract (EN)
In catalytic oxidation reaction of ß-methyl naphthalene to vitamin K3, [Mn(acac)3], [Cr(acac)3], [Ni(NO3)2] salts and Ru(II), Pd(II), Co(II), Ni(II) and Cu(II) complexes of free [N,N-bis(diphenylphosphinomethyl)aminopropylltrietoxisilane] ligand and its silica supported form syhntesized according to the reference were used as catalysts.H2O2 as clean oxidant, glaciyal acetic acid and sulfuric acid as solvent, Glass reactor, having a cooling water system wrapping around it, were used in the experiments. Efficiency of the oxidation reaction were studied on changing reaction parameters that reaction time, catalyst and H2O2 amount.
Author
Serhan Uruş
Institution
How to Cite
Serhan Uruş (Doctorate thesis). Catalytic synthesis of vitamin K3 (2-methyl-1,4-naphthoquinone), 2008, Çukurova University, Kimya Bölümü.
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