Synthesis and characterization of mixed ligands benzoilthiourea compounds with transition metal compounds
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Abstract (EN)
In this study, N,N-diethyl-N'-benzoylthiourea (HL1), N-furfuryl-N'-benzoylthiourea (HL2) and N-morpholine-N'-benzoylthiourea (HL3) ligands were obtained by reacting benzoyl isothiocyanate with diethylamine, furfurylamine and morpholine, respectively. Then new mixed-ligand copper complexes with general formulas [CuLx(bpy)]+, [CuLx(phen)]+ were sythesized with benzoylthiourea ligands (HL1-3), polypyridyl ligands (2,2'-bipyridine and 1,10-phenanthroline) and copper(II) acetate or perchlorate salts. The characterization of these compounds was elucidated by elemental analysis, NMR, FT-IR, ICP-MS, molar conductivity and magnetic susceptibility measurements. Furthermore, the thermal degradation of the complexes was investigated by thermal analysis (TG/DTA).
Author
Sait Güçlü
How to Cite
Sait Güçlü (Master Thesis). Synthesis and characterization of mixed ligands benzoilthiourea compounds with transition metal compounds, 2025, Nevşehir Hacı Bektaş Veli University.
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