Synthesis and characterization of N-carboxamide bearing sulfonamide group and its some metal complexes
2018
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Advisor: Prof. Dr. Mehmet Sönmez
Abstract (EN)
In this study, dibenzoylaceticacid-N-carboxyethylamide, which used as output substance, was obtained from the reaction of 4-benzoyl-5-phenyl-2,3-furandione with ethylurethane as reported in the literature. 2-Benzoil-N-( 4-(N-formilsulfamoil) fenil)-3-okso-3-fenilpropanamit (LH) used as the ligand was prepared from the reaction of sulfonamide with this compound. New metal complexes have been synthesized from the reaction of transition metal salts of Cu (II), Zn (II), Co (II), Ni (II) and Mn (II) as well as the ligand synthesized in the thesis. The structures of synthesized compounds were determined using by UV-Vis, FT-IR, ¹H and 13C-NMR, TGA spectroscopic techniques. In addition to spectroscopy techinques used stuctrure determination of compounds elemental analysis (C, H, N, S) method was also used.
Author
Dr. Semih Güler
Institution
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Semih Güler (Master Thesis). Synthesis and characterization of N-carboxamide bearing sulfonamide group and its some metal complexes, 2018, Gaziantep University.
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