New sandwich type and metallo phthalocyanines synthesize and characterization
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Abstract (EN)
In this work, trans-2-metoxy-4-(2-nitrovinyl)phenoxy phthalonitrile was synthesized from trans-2-metoxy-4-(2-nitrovinyl)phenol and 4-nitrophthalonitrile (1:1). Then trans-2-metoxy-4-(2-nitrovinyl) phenoxy phthalonitril were cyclotetramerized with zinco (II)acetate and cobalt(II) acetate in DMF .Lutetium phthalocyanine was prepared trans-2-metoxy-4-(2-nitrovinyl)phenoxy phthalonitrile and lutetium(III) acetate (8:1) in 1-hexanole by refluxing.Characterization of the complexes were performed by using FT-IR, UV/VIS, 1H-NMR and MASS spectroscopy.
Author
Nalan Ünüş
How to Cite
Nalan Ünüş (Master Thesis). New sandwich type and metallo phthalocyanines synthesize and characterization, 2011, Fırat University.
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