Synthesis and characterization of new methacrylamide copolymers including thiazole group
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Abstract (EN)
In this study, 2-Thiozyl Methacrylamide (TMAAm) monomer was synthesized from 2-Amino Thiazole and Methacryloylchloride in acetonitrille solvent at 70 oC in the presence of triethylamine. The structure of monomer was characterized by, FTIR, 1H-NMR and 13C-NMR spectroscopic techiques. Copolymers having various TMAAm with Glycidyl Methacrylate (GMA) and Styrene (ST) monomers having different contents were prepared in 1,4-dioxane solvent using %1 AIBN as initiator at 70 oC with the conversions below of %10. The copolymer composition were determined by elemental analysis. Monomer reactivity ratios were calculated both Finemann-Ross (F-R) and Kalen-Tüdös (K-T) methods, and a nonlinear error invariable model method with the computer program RREVM. The FTIR, 13C-NMR and 1H-NMR spectra of the copolymers were discussed. The glass transition temperature of polymers were investigated by DTA and also thermal stabilities were studied by TGA.
Author
Ece Ergül
How to Cite
Ece Ergül (Master Thesis). Synthesis and characterization of new methacrylamide copolymers including thiazole group, 2016, Uşak University.
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